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Historical Author / Public Domain Pre-1928 Public Domain

Methods and Determinations in Oil Analysis

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CHAPTER VI,

Proximate CoNsTITVUENTS AND THE MeTHops Examination axp DeTEeRMIN- ATION.

Compound Nature of Oils, Fats, and Waxes; Variations in Com- position with Circumstances of Natural Formation, _.

Methods Employed for Separa- ting Constituents, .

Determination of ' Free Fatty Acids; Free Acid Number, .

Determination of Unsapenidable Constituents, .

Determination of Water,

Adulteration of Fats with sus- pended Matters,

Sulphurised and

nstituents, .

Phoephorised

CHAPTER VIL.

Cuemicit, Reactions or Os, Fats, &c., AND THEIR Uses As Tests or Purity, &c.

Effect of Heat on Oils, Flashing Point, Characteristic Oxidation Produets,

ke. 5

pace |

rack | Action of Sulphuric Acid on Oils arkey Red Oils, . 143 Sulphuric Acid Ther- "'mal Test, MT

| Various Colour Reactions, s 151 Sulphur Chloride Reaction; V1 al canised Oils, . . 154

CHAPTER VIII.

Quanrrrative Reacrioxs oF Ous.

Keettstorfer’s Test—Total Acid 1

16 “Hg s9 2 | Practical Determination of Saponi- 123 | fication Equivalents of Glycer- 23) ides, &e., 159 12g | Proportion of Fatty Acide formed ‘by Saponification, . 163 Helmer's Test; Insoluble’ Acid | Number, . 166 Practical Determination of the | amount of Fatty Acids formed on Saponification, 167

ome ions for Anhydro Deriva- tives, Free Acids, and Unsa- ponifiable Matters, . uv

15 atben Equivalent of Fatty Acids

128; contained in Soap, . 172 Spontaneous Oxidation of Oils, Reichert’s Test and’ Modifica: Fate, te.s Hifect of Light tions thereof, . 73 thereon, . - 129! Bromine and Iodine Absorption ; Spontaneous Combustion, | | 132! Bromine Process, . 176 Film Test; Livache's Test, . |» 133) Touline Process Hubl's Test, 1179 Chemical Changes occurring dur- | Iodine Numbers of Oils, Fats, ing drying of Oils, . + 134) & 180 Elaidin Reaction ; Legler’s Cor | Acetylation’ Test; Benedikt and sistency Tester, .. « :137| Ulzer’s Test, 186 Nitric Acid Testy ss Gotouy 139. Mathyl Toaide Test; Zeisel’s Zine Chloride Reaction and Colour + 191 Test; Action of Zine Chloride Tabulated results of the various on Oleic Acid, . # . 141, Quantitative Tests, . . 194

$4, Processes Used for Extracting, Rendering, Refining, and Bleaching Oils, Fats, &c.

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